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We report an exclusively tandem C—O and C—C bond forming beyond the esterification and cyclization reaction of 2‐acylbenzoic acids with alcohols to regio‐ and stereoselective synthesis of the (Z)‐3‐ylidenephthalides. The reaction uses the nontoxic, inexpensive H3PMo12O40 as catalyst and produces water as the sole by‐product, making the reaction environmentally benign and sustainable. Moreover, this...
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