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A new layered aluminophosphate named Mu-4 was recently obtained from a quasi non-aqueous mixture involving mainly diethylformamide (DEF) as solvent in addition to limited amounts of water. During the synthesis, DEF is decomposed and the resulting protonated diethylamine is occluded in the as-synthesized material, neutralizing the negative charge of the inorganic layers. The structure consists of anionic...
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