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The 1,3‐dipolar cycloaddition of activated internal alkynes with azides has been developed into an efficient polymerization reaction for constructing functional linear 1,4,5‐trisubstitued polytriazoles. However, it is rarely employed for the synthesis of hyperbranched polymers. In this work, metal‐free polycycloadditions of tris(3‐phenylpropiolate)s (1) and tetraphenylethene‐containing diazides (2...
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