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The isotypic aluminium stannides Ln9Al5Sn10 (Ln = Yb, Eu) are the first ternary compounds in the systems Yb‐Al‐Sn and Eu‐Al‐Sn. They were synthesized in the course of systematic experimental work on the phase stability along the sections LnAl2 – LnSn2 from the elements at maximum temperatures of 1170 K. Their crystal structures were determined using single‐crystal X‐ray diffraction [both monoclinic,...
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