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In this paper, we reported the synthesis of single-crystalline octahedral LiMn 2 O 4 particles by a two-step method in which well-shaped octahedral Mn 3 O 4 was easily obtained by the hydrothermal reaction of KMnO 4 in water/N, N-dimethyl formamide (DMF) mixed solution and then transferred to LiMn 2 O 4 by the solid-state lithiation process....
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