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Here we report the synthesis and characterization of anatase TiO2 powders by the double-nozzle electrospray pyrolysis method. Titanium(IV) bis(ammonium lactato) dihydroxide (TALH) aqueous solution (2.0 wt%) and pure H2O were separately injected into capillaries by using two syringe pumps, and were electrosprayed by using positive (+4 kV) and negative (−4 kV) DC voltage, respectively. Under a stream...
By using the droplet-fixation method, quantitative analyses of the size and dispersion state of electrosprayed droplets were conducted. At first, titanium(IV) bis (ammonium lactate) dihydroxide (TALH) aqueous solution (2wt%), as a precursor of TiO 2 , was electrosprayed using single-nozzle setting, and the electrospray parameters were optimized. Fine and monodispersed droplets (5.00μm with...
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