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In this work, we report the results of in situ Raman monitoring of copper zinc tin sulfide [Cu 2ZnSnS4 (CZTS)], phase under relevant processing conditions at elevated temperatures. CZTS films are prepared from a simple sol-gel method, followed by sulfurization. Raman microspectroscopy measurements are carried out using a 514.5-nm excitation laser on CZTS samples at room temperature and under in situ...
Copper zinc tin sulfide Cu2ZnSnS4 (CZTS) thin film and powder samples are successfully prepared using a simple sol-gel sulfurization procedure. The samples were characterized using ex situ techniques such as XRD, SEM, EDS. In addition, advanced in situ Raman micro-spectroscopy characterization of CZTS material from room temperature to 650 °C was demonstrated for the first time. Preliminary results...
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