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The morphology of polyurethane (PU)–poly(methyl methacrylate) (PEMA) interpenetrating polymer networks (IPNs) were investigated by means of small-angle X-ray scattering (SAXS) and modulated-temperature differential scanning calorimetry (M-TDSC) techniques. Based on the analysis method employed by Tan et al. [Polymer 1997;38:4571], the interfacial thickness in the IPNs was calculated from SAXS data...
The glass transition behaviour and morphology of 70:30 polyurethane–poly(ethyl methacrylate) (PU–PEMA) interpenetrating polymer networks (IPNs) in which the crosslink density in both networks was systematically varied were investigated by means of modulated-temperature differential scanning calorimetry (M-TDSC) and dynamic mechanical thermal analysis (DMTA). The observed influence on the glass transition...
A modulated-temperature differential scanning calorimetry (M-TDSC) method for the analysis of interphases in multi-component polymer materials has been developed further. As examples, interphases in a polybutadiene-natural rubber (50:50 by mass) blend, a poly(methyl methacrylate)-poly(vinyl acetate) (50:50 by mass) structured latex film, a polyepichlorohydrinpoly(vinyl acetate) bilayer film, and polystyrene-polyurethane...
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