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A copper and silver‐promoted intermolecular 1,2‐alkylarylation of styrenes with α‐carbonyl alkyl bromides and arenes for producing highly bulky 1,1‐diarylalkane derivatives has been developed. In this transformations, two new C−C bonds were formed in a single reaction step through C−Br bond cleavage and C(sp2)−H functionalization. This protocol tolerates a variety of α‐carbonyl alkyl bromides, including...
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