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Macrotetrolide α (1), a designed polynactin analog composed of (+)- and (−)-bishomononactic acids, was synthesized. The monomeric acids were prepared using cis-selective iodoetherification and optical resolution of the corresponding O-acetylmandelates as the key steps. Esterification and macrolactonization of the monomers were performed by Corey–Mukaiyama–Gerlach method. Compound 1 showed no immunosuppressive...
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