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A polyvinylpyrrolidone (PVP)-assisted synthesis method was reported to prepare monodisperse UiO-66 octahedral crystals with tunable sizes. In this acetic acid/PVP co-modulated synthesis system, the relatively weak coordination of PVP to Zr(IV) played an important role in manipulating the sizes of UiO-66 crystals instead of their shapes. With the optimized PVP concentrations, sizes of the monodisperse...
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