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Alternating benzene–heteroaryl oligomers possess fascinating optoelectronic properties and a wide range of applications. This article presents the facile synthesis of benzene–pyrrole oligomers with diverse functional groups and the elongated alternating heterocycle–benzene–pyrrole oligoaryls. The syntheses are based on a one‐pot, three‐step reaction of propargylic dithioacetals and imines. The subtle...
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