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M-ZnS (M=Cr, Cu, Ni, Mo and Ag) photocatalyst arrays were rapidly screened for photoelectrochemical water oxidation using scanning electrochemical microscopy (SECM) with an optical fiber. Among the various arrays, the spot with the precursor composition Ni0.1-Zn0.9S showed the highest photocurrent in 0.1M Na2SO4/Na2SO3 solution under both UV-visible and visible light irradiation. X-ray diffraction...
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