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The applicability of ATR-FTIR for the determination of the HDO content in heavy water (D2O) was investigated. Two groups of calibration standard solutions, of low contents (0–1 n% H2O in heavy water) and of higher contents (0–10 n% H2O in heavy water) were prepared by adding properly calculated amount of H2O to D2O by weight. The absorbances at 3400 cm−1 (ν, O–H) against the calibration standards...
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