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Pt nanoparticles were prepared by the chemical reduction method. The average diameter of Pt nanoparticles was determined to be 2.5 nm by TEM. The electrochemical properties of Pt nanoparticles were studied by cyclic voltammetry. In comparison with massive Pt, the oxidation current peak of CO adsorbed on Pt nanoparticles is broader. Twin adsorbates of CO on Pt nanoparticles were determined by in situ...
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