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Dispersed Pd nanoparticles (Pdπ) have been synthesized by reducing H2PdCl4 with ethanol, and stabilized using poly(vinylpyrrolidone) (PVP). The Pdπ is applied to the glassy carbon substrate to form a thin film, and then the potential cyclic scanning at 50 mV-s−1 from -0.25 to 1.25 V was carried out for about 30 min to form the aggregations of Pdπ (Pd agπ ). FTIR spectroscopy of both transmission...
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