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The one‐pot combination of enzymatic ring‐opening polymerization (eROP) and ring‐opening metathesis polymerization (ROMP) is successfully established to construct block copolymers. cis‐1,4‐Diacetoxy‐2‐butene is employed both as a precursor to initiate eROP of ε‐caprolactone or 15‐pentadecanolide and as a chain transfer agent in ROMP. The obtained polymers are systematically characterized by NMR, GPC,...
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