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A series of poly(thiophene) derivatives with decyl‐oligo(oxyethylene) side groups, (PDnET) is synthesized via oxidative coupling polymerization. PD3ET and PD4ET with longer oligo(oxyethylene) units exhibited a liquid crystalline phase with well‐ordered lamella structures, although PD3ET showed a more ordered structure than PD4ET. PD1ET and PD2ET have shorter oligo(oxyethylene) groups than PD3ET and...
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