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Single‐crystalline grains and grain boundaries in an as‐grown molybdenum disulfide monolayer are visualized by second‐harmonic‐generation microscopy. Further statistical analysis reveals that the boundary formation is driven by kinetics, rather than energetics. The method and derived growth mechanism described on page 4069 by S. W. Wu and co‐workers can be extended to many other 2D materials and help...
Grain boundaries in as‐grown polycrystalline MoS2 monolayers are revealed by second‐harmonic‐generation microscopy. Through the anisotropic polarization pattern and phase interference at the grain boundary, grain edge termination and boundary types are identified. Statistical analysis on hundreds of grains shows that grain‐boundary formation is driven by kinetics and can be nicely described by the...
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