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Herein, Non-noble bimetallic CoNi nanoparticles encapsulated within h-BN (CoNi@h-BN) is successfully synthesized via annealing freshly prepared metal ammine boride complexes [Co0.5Ni0.5(NH3)6]Cl3)/NH4BO2 and KBH4 under flowing nitrogen gas at 900 °C for 2 h. The result showed that CoNi nanoparticles with general size of 17 nm completely encapsulated by h-BN shells, and the h-BN shells on the CoNi...
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