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The triazine hindered amine (THA) nitroxide radicals are important to the preparation of halogen‐free flame retardants, but the traditional methods using peracetic acid was limited in further sustainable development in industry. In this work, the bicarbonate‐activated hydrogen peroxide system with ethyl acetate as the solvent (BAP‐EA system) was firstly employed in TH‐7 nitroxide radicalization, which...