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Quantitative β-boration of α,β-unsaturated carbonyl compounds was achieved utilizing the eco-friendly solvent EtOH along with MeOH at room temperature in 1 h, by a CCC-NHC pincer Rh complex mixture. Substrates with β-substituents were successfully converted yielding challenging, quaternary C–B bonds. The air- and water-stable pre-catalyst A, identified as a mixture of iodo and chloro CCC-NHC pincer...
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