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The use of high-resolution magic angle spinning NMR spectroscopy for in situ studies of low-molecular-mass compounds in red algae has been studied. The impact of different acquisition parameters on the resulting T 2 -filtered one-dimensional high-resolution magic angle spinning 1 H NMR spectra is described. The technique was used for in situ identification and quantification of some...
A sensitive and selective method for detection and quantification of 1,5-anhydro-d-fructose, microthecin, and 4-deoxy-glycero-hexo-2,3-diulose using GC-MS in selected ion monitoring mode has been developed. These compounds, which occur in many biological systems, have here been quantified in the red algaGracilariopsis lemaneiformis.A screening of other algae showed the occurrence of 1,5-anhydro-d-fructose...
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