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The extraction of chemical shift anisotropy (CSA) tensors of protons either directly bonded to 14N nuclei (I=1) or lying in their vicinity using rotor-synchronous recoupling pulse sequence is always fraught with difficulty due to simultaneous recoupling of 14N–1H heteronuclear dipolar couplings and the lack of methods to efficiently decouple these interactions. This difficulty mainly arises from the...
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