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High‐performance thermoelectric BiCuSeO ceramics have been prepared by solid state reaction combined with plasma activated sintering (PAS). Phase compositional and microstructural studies indicate composites having refined grain sizes (600–700 nm) with nanostructured ZnSe secondary phase. Our results reveal that Zn doping can lead to a large change in the carrier concentration (from 0.036 × 1020 cm...
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