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By controlling the reactant ratios, hydrothermal time, hydrothermal temperatures, pH values of the prepared solutions, and the concentrations of K3C6H5O7·2H2O, 1 mol% Eu3+ doped cubic phase of K5Gd9F32 and/or orthorhombic phase of GdF3 micro/ nanocrystals have been synthesized based on a hydrothermal method. For comparison, the sample was also synthesized by a co-precipitation method. The samples...
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