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Perovskite CaTiO 3 has three polymorphic phases: cubic, tetragonal and orthorhombic. The present article deals with the first time preparation of nanocrystalline orthorhombic polymorphs of CaTiO 3 by high energy ball milling the equimolar mixture of CaO and anatase (a)-TiO 2 powders. It has been observed that a small amount of CaTiO 3 is formed just after 1h of ball...
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