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An iridium complex [H(dmso)2]2[IrCl6] (1) is synthesized via the reaction of H2IrCl6 with DMSO in an acetone solution. The substance is thoroughly characterized using UV‐Vis, ATR‐FTIR, NMR, and EPR spectroscopies, single‐crystal and powder X‐ray diffraction. Iridium undergoes a slow spontaneous reduction to the chemical state +3 when solutions of 1 in water, hydrochloric acid, or acetone (CIr=n ⋅...
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