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A Ni-Zn binary metal coating was electrochemically deposited on a copper electrode that was coated with nickel (bottom layer). This was then etched in concentrated alkaline solution (30 wt% NaOH) to produce a nanoporous Ni electrocatalytic surface for borohydride electro-oxidation in alkaline solution. The bulk and surface compositions of the coating before and after alkaline leaching were determined...
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