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The cyclopentadienyl complex Cp*Ir(PMe3)Cl2 reacts with the dipotassium salt of phthalic acid in the presence of AgPF6 via chloride substitution to give the ortho-metalated compound Cp*Ir(PMe3)[C6H3(CO2)(CO2H)]. This new compound has been isolated by recrystallization and has been characterized in solution by 1H and 13C NMR spectroscopies, and the solid-state structure has been verified by X-ray crystallography...
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