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Prismatic vermilion single crystals 200µm–2mm in size, together with a white powder, were obtained by heating a mixture of binary nitrides containing Mg3N2 at 2030°C under 0.85MPa of N2. Yellow, thick-platelet single crystals with sizes of 150–500µm were also found to grow at or near the surface of the product. Single crystal X-ray diffraction demonstrated that the vermilion crystals were orthorhombic...
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