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Coulostatic potential transients induced by nanosecond pulsed laser irradiation on Pt(111) stepped surfaces in perchloric acid solutions are analyzed here. The results provide unique information on the effect of the structure of the metal surface on the potential-dependent water reorientation at the electrified interphase. The most significant information is obtained from the sign and shape of the...
A thermodynamic method based on the work done by Frumkin and Petrii [A.N. Frumkin, O.A. Petrii, Electrochim. Acta 20 (1975) 347], to calculate the so-called double layer capacity for a Pt(111) electrode is proposed. The analysis requires careful measurement of the total charge density versus potential curves for a series of solutions with composition (0.1−x)M KClO 4 +xM HClO 4 . A...
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