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This work demonstrates the formation of self‐ordered double‐walled ZrO2 nanotube array via electrochemical anodization in glycerol‐based electrolyte. Compared with its counterpart of single‐walled ZrO2 nanotube array, the tube wall of double‐walled ZrO2 nanotube split into outer and inner layers for the decomposition of glycerol during anodization process. Moreover, the double‐walled structure showed...
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