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The effect of heating and cooling rates on the DSC (differential scanning calorimetry) heat flux peak of the monoclinic-tetragonal transition of zirconia was investigated in the 0.4–20°C/min scan rate range. While the peak position, shape and area at high to moderate scan rates are consistent with existing literature data, a ‘step change’ (i.e., a peak-less baseline shift) was observed for the extremely...
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