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Mesoporous Ni–P amorphous alloy nanospheres with controllable sizes and compositions were synthesized by chemical reduction of Ni(OH)2 colloidal particles co-assembling with surfactant hexadecyl-trimethyl-ammonium bromide in liquid crystal mesophase using hypophosphite as reductant. The effects of the synthesis conditions on the particle size, composition and mesostructure of the mesoporous Ni–P nanospheres...
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