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MoS 2 was prepared by thermal decomposition of ammonium tetrathiomolybdate in inert gas at 723–773 K and activated by procedures involving evacuation at 723 K and/or reduction at different temperatures, predominately 573 K. Bulk and surface properties of these samples were studied by X-ray diffraction (XRD), extended X-ray absorption fine structure (EXAFS), X-ray photoelectron spectroscopy...
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