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Asimicin (1) exhibits potent antitumor activity and comprises a central C2‐symmetric bis‐tetrahydrofuran and two aliphatic side‐chains, one of which terminates with (S)‐methyl‐2(5H)‐furanone. This work reports a convergent total synthesis of 1 in 17 steps from d‐gulose derivative 4. Decarbonylative radical‐radial homo‐coupling of α‐alkoxyacyl telluride 12 a efficiently produced the C2‐symmetric core...
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