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A recent clinical trial assessing human autonomic cardiovascular regulation applied pacemaker channel inhibition with ivabradine, norepinephrine transporter blockade with reboxetine, and beta-adrenoreceptor blockade with metoprolol. To verify patient adherence, we developed and validated a fast UPLC–MS/MS assay measuring all three compounds simultaneously. Deuterium-labeled drugs, d 3 -ivabradine,...
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