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High-energy ball milling was used to promote the solubilization of iron into NiAl powder for an iron concentration range of 10–30 wt.%. The microstructural evolution induced by the intense mechanical deformations, under different milling conditions, was followed by X-ray diffraction and Mössbauer spectroscopy. The Mössbauer spectra are dominated by a magnetic sextet of about 33 T. Increasing the time...
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