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An efficient method for improving the catalytic properties of unsupported Ni/MoS2 catalysts is mixing thiometalate precursors applying the appropriate precursors and thermal conditions. High active catalysts for the hydrodesulfurization (HDS) of dibenzothiophene (DBT) are prepared by the controlled decomposition of physical mixtures of Ni(diethylentriamine)2MoS4 (NDTA-TM) and [(Propyl)4N)]2MoS4 (TPA-TM)...
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