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Monolithic materials were synthesized in capillaries by in situ polymerization with N‐isopropylacrylamide, glycidyl methacrylate, and ethylene dimethacrylate as the monomers, and methanol and PEG as the porogens. With γ‐alumina nanoparticles attached to the surface of the porous monolithic column via epoxide groups, a novel polymer monolith microextraction (PMME) material was prepared with a good...
DOI: 10.1002/jssc.201300754Monolithic materials were synthesized in capillaries by in situ polymerization. With γ‐Al2o3 nanoparticles attached to the surface of the porous monolith via epoxide groups, a novel polymer monolith microextraction material was prepared with good mechanical stability and high extraction capacity. The SEM micrographs clearly demonstrated that the pores and size of the microglobules...
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