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Alumina-supported Pd–Sn catalysts prepared by successive impregnation of the precursors, calcination, and reduction contain SnO 2 and SnAl 2 O 5 , Pd–Sn solid solutions, and intermetallic phases Pd 2 Sn and Pd 3 Sn. The formation of Pd 3 Sn is favored not only by lowering the Sn/Pd ratio but also by introducing tin through ethanolic impregnation. The...
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