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Here reports an photoinduced glycosylation of trichloroacetimidate donors and several alcohols using 3,11‐dimethoxydinaphthothiophene as an organo Lewis photoacid catalyst upon long‐wavelength UV‐LED light (385 nm) irradiation. The reaction proceeded under mild reaction conditions smoothly to give the corresponding glycosides in good to high yields. In addition, the present glycosylation method was...
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