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A simple and easy method for chemoselective synthesis of hexopyranosyl acetates and 2,3-disubstituted tetrahydropyrans from hex-2-enopyranosyl acetates was demonstrated. The former was achieved by hydrogenation catalyzed by Rh/Al 2 O 3 in EtOAc/toluene solvent at 0°C, while the latter was carried out using Pd/C in EtOH/AcOH at 25°C.
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