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1-Aryl-3,4-dihydroisoquinolines undergo smooth acetoxylation/alkoxylation in the presence of 5mol% Pd(OAc) 2 and a stoichiometric amount of PhI(OAc) 2 by means of C–H activation to produce the corresponding acetoxy- and alkoxy-1-aryl-3,4-dihydroisoquinoline derivatives respectively in good yields with high regioselectivity. It is a first example on oxidative functionalization of arenes...
Indoles undergo smooth cyanation with CuCN in the presence of 20mol% Pd(OAc) 2 and 40mol% CuBr 2 in DMF to produce a wide range of the corresponding 3-cyanoindoles in good yields with high regioselectivity.
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