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α‐Hydroxyamide is an important chemical component widely observed in biologically active natural products. One of the most direct methods to access a α‐hydroxyamide is the Passerini‐type reaction. However, this catalytic process was limited. Herein, we report the first examples of 3,5,6‐trifluoro‐2‐pyridone‐catalyzed α‐addition of isocyanides to aldehydes, in the presence of water in benzene, to provide...
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