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Mesostrukturierte MFI‐Nanoschichten kristallisieren in der Hydrothermalsynthese nicht‐topotaktisch über eine schichtartige Silicatzwischenstufe. Festkörper‐2D‐NMR‐Analysen mit dynamischer Kernpolarisation (DNP) liefern direkte Belege, dass die intermediären schichtförmigen Silicatbausteine und das kristallisierende Netzwerk von MFI‐Nanoschichten die gleichen kovalenten 29Si‐O‐29Si‐Bindungen aufweisen...
Mesoporous zeolites are a new and technologically important class of materials that exhibit improved diffusion and catalytic reaction properties compared to conventional zeolites with sub‐nanometer pore dimensions. During their syntheses, the transient developments of crystalline and mesoscopic order are closely coupled and challenging to control. Correlated solid‐state NMR, X‐ray, and electron microscopy...
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