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The mechanism of dimethyl carbonate (DMC) formation from CO2 and methanol is investigated using three well-shaped CeO2 catalysts, nanorod, nanocube and octahedron, which are packed with different crystal planes. In situ Fourier Transform Infrared Spectroscopy (FTIR) is employed to probe each reaction step in the DMC synthesis. The number of OH groups and the species of CO2 adsorptions on ceria surface...
This paper describes the effect of the in situ hydrolysis of 2-cyanopyridine and its derivatives on the synthesis of dimethyl carbonate (DMC) from CO2 and methanol over CeO2. 2-Cyanopyridine, with the highest electronic charge number of the carbon in the cyanogroup, is the most effective agent to accelerate the desired reaction by a decrease of water. CeO2 (110) planes are active for the hydrolysis...
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