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The complex 2(C8H10N4O2).[Co(H2O)4(NCS)2].4H2O was prepared in the water-ethanol solution at room temperature and characterized by the single crystal X-ray diffraction analysis, 1H, 13C NMR, TGA/DTA and IR spectroscopy. This complex was crystallized in the monoclinic system (P 21/c). The unit cell parameters are a = 10.65854 (19) A°, b = 8.16642 (14) A°, c = 18.0595 (3) A° with β = 96.4701° (15)....
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