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A family of rare earth antimonide oxycarbides have been prepared and structurally characterized. These superlattice phases are constructed from NaCl‐type RESb slabs sandwiched between RE–O–C layers. Depending on the carbon content and synthetic conditions, three different RE–Sb–O–C structures can be obtained. At lower temperatures,RE9–δSb5(O,C)5 phases are obtained for RE = La, Ho. These phases adopt...
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